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Chemical constituents from rhizomes of Polygonum suffultum
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- Author:
- No author available
- Journal Title:
- CHINESE TRADITIONAL AND HERBAL DRUGS
- Issue:
- 8
- DOI:
- No doi available
- Key Word:
- 红三七;蓼属;三萜
Abstract： 目的 研究民间药红三七(支柱蓼Polygonum Suf fultum的根茎)的化学成分.方法 运用溶剂萃取、硅胶柱色谱、聚酰胺柱色谱、凝胶柱色谱以及大孔吸附树脂柱色谱、重结晶等方法分离纯化,根据核磁共振谱数据及与对照品共薄层色谱鉴定化合物的结构.结果 从红三七乙醇提取物中分离鉴定了11个化合物:3β-羟基-新何帕-13(18)-烯(1)、3β-乙酰氧基-新何帕-13(18)烯(2)、3p-乙酰氧基何帕-17(21)-烯(3)、没食子酸(4)、谷甾醇(5)、胡萝卜苷(6)、木栓酮(7)、绿原酸正丁酯(8)、杨梅素-3-O-β-D-葡萄吡喃糖苷(9)、绿原酸(10)和4-O-咖啡酰基奎宁酸(11).结论 除化合物4外,以上化合物均为首次从红三七中分离得到,其中化合物1～3、8、9、11系首次从蓼属植物中分离得到.化合物1和2为新天然产物.
- [1]王开金,张颖君,杨崇仁.蓼属植物的化学成分与生物活性研究进展[J].2006,(1).
- [2]苏艳芳,邸利芝,吕敏,等.花木蓝根的化学成分研究[J].2008,(11).
- [3]崔 宝良,中村 基之,金城 順英,等.Chemical Constituents of Astragali Semen[J].1993,41(1).
- [4]Nakatani N,Mitani T,Kikuzaki H,etc.Identification, quantitative determination, and antioxidative activities of chlorogenic acid isomers in prune (Prunus domestica L.).[J].2000,48(11).
- [5]郭增军.陕西七药[M].2003.
- [6]Zhu XD,Wang WF,Ju P,etc.Phenolic compounds from Viburnum cylindricum[J].2005,88(2).
- [7]Tomoki Tatefuji,Tsunetaka Ohta,Masao Ikeda,etc.Isolation and Identification of Compounds from Brazilian Propolis which Enhance Macrophage Spreading and Mobility[J].1996,19(7).
- [8]Ban JY,Nguyen HTT,Lee HJ,etc.Neuroprotective properties of gallic acid from Sanguisorbae radix on amyloid beta protein (25-35)-induced toxicity in cultured rat cortical neurons[J].2008,31(1).
- [9]吕敏,苏艳芳,高媛,等.苏木蓝和花木蓝的化学成分研究[J].2009,(3).
- [10]B. Achari,Anjana Pal,S.C. Pakrashi.Studies on indian medicinal plants. Part XXXVI: New D:E-cis neohopane derivatives from alangium lamarckii[J].1975,16(48).
- [11]Muhammad Ali,Irfanullah,Sarah Bibi.Spectral Assignments and Reference Data[J].2001,39(7).
- [12]Oksuz S. Serin S..Triterpenes of Centaurea Ptosimopappoides[J].1997,46(3).
- [13]Ajit K. Chakravarty,Kazuo Masuda,Hideki Suzuki,etc.Unambiguous assignment of 13C chemical shifts of some hopane and migrated hopane derivatives by 2D NMR[J].1994,50(9).
- [14]段营辉,戴毅,高昊,等.草珊瑚的化学成分研究[J].2010,(1).